Method and apparatus for accelerating maturing of distillates
专利摘要:
A process for acceleration of the ripening of spirits is described, wherein the spirits are irradiated with ultrasonic radiation in the presence of wood staves which serve as a source of bouquet-improving additives. Through control of the irradiation parameters, reproducible results may be achieved on the industrial level. Circulation of the spirits within the irradiation chamber increases the uniformity of the irradiation. An apparatus is described for a continuous performance of the process on an industrial level. 公开号:SU966114A1 申请号:SU787770408 申请日:1978-12-27 公开日:1982-10-15 发明作者:Клаус Дудар;Эвальд Зелигер;Гертрауде Хюбнер;Вилгелм Банзе 申请人:Феб Ратионализирунг (Инопредприятие); IPC主号:
专利说明:
; (d) METHOD FOR ACCELERATING DISTILLATE MATERIALS AND DEVICE FOR ITS APPLICATION one The invention relates to methods and devices for accelerating the maturation of distillates by means of an ultrasonic treatment. Characteristics of known technical solutions. For the production of horses and bread vodka, their maturation or aging is achieved through the long storage of distillates in oak tanks or metal tanks with an oak wood accelerator. This method is associated with high costs of time and capacity, since the aging process lasts from many months to several years. Known solutions that reduce the natural aging process. Along with carbonation with ozone, oxygen, nitrogen or their mixtures with simultaneous ultraviolet treatment, short-term treatment in vibrational mills, heat treatment with electric current, ultrasonic distillates are known to be treated in the presence of taste-stimulating accelerators. A method is known for the rapid maturation of distillates (DD PS 614) and ultrasonic treatment (CH) PS, in which ultrasound, along with the acceleration of chemical reactions, also accelerates extraction processes in the presence of bunch-forming accelerators, mainly wood. A disadvantage of the known methods of processing by ultrasound is that they do not achieve reproductive quality parameters, Tc (as the most important technical and technological conditions are not fulfilled.
权利要求:
Claims (1) [1] The purpose of the invention is to develop an industrial method that accelerates the maturation of distillates and by which reproductive quality parameters are achieved. 3E The invention has the task to develop an industrial method with the necessary devices for use, the introduction of which significantly accelerates the maturation of distillates with at least the same quality remaining. This goal is achieved by the fact that distillates in the presence of bouquet-forming accelerators, mainly wood, are exposed to an ultrasonic field with a possible uniform distribution of intensity throughout the whole volume and the optimum operating frequency. In order to achieve an absolute equal to the magnitude of the ultrasonic action: on all elements of the distillate volume. It is pumped at the time of dubbing in the system being voiced. In this case, the distribution of the distillate flow and the location of wood accelerators are important. The method is applied in a closed system, isolated against the heat transfer, i.e. approximately adiabatically. Since the introduced ultrasound energy and the temperature increase associated with it are found in: depending on the degree of maturation of the distillers, a comparative temperature control is possible by means of adiabatic and replenished capacity. In this case, the quantitative dependence of the temporal energy and the increase in temperature associated with it depends on the type of distillate. The accuracy of the measured temperature should be + 1/10 СC. To reduce the input energy with a uniform effect, the medium being sounded is under increased static pressure. This static pressure is realized by compressing the gas over the medium being sounded and stands in certain ratios to the sound intensity. As a result, the cavitation effect rises by several orders of magnitude. It was found that using the method for distillate maturation achieves very high time savings with very good quality of the final product with the following parameters: Ultrasonic frequency, kHz, 20-50, mostly 35 kg. Specific sound power, W / l1.7 Average sound intensity, W / cm 0,5 Wood accelerator surface depending on the type of distillate, Transfer cycle, hours 3 The given ultrasound parameters are optimal and, together with those for the corresponding distillate, having voiced and a surface of wood or accelerator guarantee flowing under the control of the process of chemical reactions in a complex with buketoobrazuyuschimi substances. An embodiment of the invention. The invention should be explained in more detail in an exemplary embodiment of the invention. FIG. 1 schematically shows a device that implements the proposed method; in fig. 2 - the same, cross section; in fig. 3 - voiced capacity, a section in FIG. k - device for capsular vibrations and wood accelerators, section. The device for carrying out the proposed method consists of two equipped with 8 capsule oscillators 8 voiced containers, which are simply alternately voiced or to prevent the time caused by the technology. are emptied and filled,. Both voiced containers 1 are the main module of the Ultrasonic device. The number of these containers can be increased, if necessary, through free terminals 12 and 13. Ultrasonic energy required for processing is generated by ultrasonic generators 22. / 1p controlling the optimal mode of ultrasonic generators 22 between them and oscillators 8 turns on the device for measuring ultrasonic power i the value of the power delivered by the ultrasonic generator and the associated small scatter of sound intensity are very important in this method of distillates maturation quality parameters The dot intensity of the ultrasound can be measured by a special probe through the opening 9, and its value indicates the intensity measurement instrument associated with the probe. In adiabatically made voiced capacitance x 1, two are provided. cavity, and between the inner 2 and outer 3 cavities there is a space filled with insulating material i. The covers hermetically cover the voiced containers 1. On the covers 5, the holder 6 for wood accelerators -7 and capsular vibrations 8 are fixed so that a uniform sound field is created in the media 2t and the wood accelerators 7 are voiced without sound from all sides. Capsular oscillators 8 are fixed by means of pipes 25 to a removable manhole cover 18 so that each capsule oscillator can be removed from the installation without affecting the operation of other oscillators. Through pipes 25 to piezoceramic transducers with on (high frequency cables 26 are laid with the clutches. I The pump 11 carries out through the inlet or drain 27, depending on the position of the crane, filling or emptying the containers 1, and pumping alcohol 2k during the process sounding In the pipeline between the pump 11 and the inlet opening 21 of the tank, the indicator 19 of the fluid current is installed. To distribute the tank evenly, there is a distribution plate 10 located after the filling hole. There is an optimal pressure setting device for protection against sudden pressure increases in the containers on the lids 5. Bringing through the valve 16. The supply of the finished product 2k is additionally possible through the valve 20. Claim 1: Method for accelerating the maturation of distillates under by the action of ultrasound in the presence of bouquet-forming accelerators, mainly wood, n (these distillates serve as a transmission medium for ultrasonic waves, differing from the fact that the treated distillate is in a closed system and continuously stirred for 30-60 minutes, exposed to a homogeneous throughout the volume of a powerful sound field with a maximum value of 1.7 W / l, with a frequency of 20 to 50 kHz, mainly 35 kHz, sound intensity with a maximum value of 0 , 5 W / cm- and the surface of the wood accelerator depending on the type of distillate, 20-CO cm / l with a replating cycle of 3-4 m. 2. A method according to claim 1, characterized in that the medium being sounded is under the static pressure of a compressed gas with a maximum value of 6 kpd / cm, the value of which consists in certain ratios with sound intensity, and also because the amplification of the cavitation effect reduces the amount of energy introduced with the main technological parameters remaining unchanged, 3 "Device for applying the method according to claims. 1 and 2, characterized in that the two voiced containers, 1, equipped with capsule oscillators 8, are made adiabatically so that between the internal cavity 2 and the external cavity 3 there is a space filled with an insulating material, and the containers are closed with the help of covers 5 with holders 6 for wood accelerators 7 and capsule oscillators 8, fixed so as to provide, as far as possible, a uniform sound field in the medium being voiced 24. 4. The device according to claims. 1-3, characterized in that the pump 11 pumps the distillate 24 to achieve sounding of all volume elements and continuously mix through the liquid flow meter 19 to the filling opening 21 with the distribution plate 10 dll of the distribution of the distillate B current, cycle, and further According to the position of the crane, it allows through the filling opening 21 or the drain 27 and 20, respectively, to fill and empty the sounded capacitor 1, and the filling level is monitored by means of a measuring device 17 .5 The device in PP. I-, which is different from the fact that ultrasound energy is needed for articulating, Zym of ultrasonic generators 22 through high-frequency cable 26 to oscillators 8, and between the ultrasound source and the consumer, an ultrasonic power measuring device 23 is in operation. It is recognized as an invention according to the results of the examination carried out by the Office for the Invention of the German Democratic Republic. П 10 21 U / /. S 25
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同族专利:
公开号 | 公开日 US4210676A|1980-07-01| IT7947829D0|1979-01-30| FR2416265A1|1979-08-31| DD134779A1|1979-03-21| DD134779B1|1981-02-25| RO76515A|1981-11-04| IT1164660B|1987-04-15| DE2902114A1|1979-08-02| JPS54119098A|1979-09-14| ES477330A1|1979-07-01|
引用文献:
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申请号 | 申请日 | 专利标题 DD20350378A|DD134779B1|1978-02-01|1978-02-01|METHOD AND DEVICE FOR ACCELERATING THE RIPENING OF SPIRITS| 相关专利
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