• 专利附录
  • 专利说明
  • 权利要求
  • 类似技术
  • 同族专利
  • 引用文献
  • 法律状态
  • 优先权
    • 专利摘要:
    A process of continuously forming pH modified protein filaments from a proteinaceous material is disclosed wherein an aqueous slurry of the proteinaceous material is formed having a proteinaceous solids content of between about 0.5 and 35% by weight. Discrete filaments are formed by conducting the slurry under pressure through a heat exchange zone and heating the slurry to a temperature which is above 240 DEG F. whereby the protein is subjected to such temperature for a sufficient period of time so that elongated filaments are thereafter separated from the remaining constituents of the slurry. The heated slurry is then continuously removed from said heat exchange zone through a back pressure creating orifice whereby discharge of said filaments from the heat exchange zone to a collecting zone is controlled by confining the stream of said filaments to within a total angle of between about 4 DEG and 90 DEG . A pH elevating material is then injected into the stream of filaments during confinement in order to modify the pH of the filaments to a pH of above about 6.0 and preferably between about 6.0 and 7.0. It has been determined that pH modified filaments produced in the above manner are highly functional for meat extender applications, yet pH modification in the above manner provides the maximum yield of protein filaments from a given weight of proteinaceous slurry since the pH of the slurry is not altered prior to filament formation.
    公开号:SU921450A3
    申请号:SU762426457
    申请日:1976-12-02
    公开日:1982-04-15
    发明作者:Энтони Хоер Ральф；Хенри Стюарт Майкл
    申请人:Ральстон Пьюрина Компани (Фирма)；
    IPC主号:
    专利说明:

    The invention relates to techniques for the production of protein fibers from protein material used for additives to meat products in the food industry. b
    There is a known method for producing a protein food product, which consists of preparing a suspension of defatted soybeans, adding HC to pH 4.3, the resulting precipitate is dried, added to the initial precipitate in an amount providing 35% humidity, the pH is adjusted to 7, and the resulting mixture is fed to an extruder, at the exit of which the protein fibers have a temperature of -5 150 ° C [1].
    There is also known a method for producing protein fibers, comprising preparing an aqueous suspension from plant materials, heating the suspensions by passing through a heat exchanger with a solids content of 0.5-35 wt.%, Forcing the heated suspension through a diaphragm under a pressure of 25 to obtain protein fibers and unloading fibers into the collection area [2].
    Formed protein fibers are widely used in the production of a wide variety of food products with improved aesthetic properties and taste.
    However, these known methods do not involve adjusting the pH of the suspension prior to the formation of fibers. in the desired range from 6.0 to 7.0, as a result of which these wafers cannot be used as a source of additives to foods such as meat. Protein fibers having a pH in the range of 6.0 to 7.0 have better culinary properties when added to meat than those having a lower pH of 4.5 to 5.5.
    The closest to the proposed technical essence and the achieved result is a method of producing protein fibers, which provides for the preparation of an aqueous suspension of a dilute protein-containing raw material having a pH of 4.5-5.0 with a solid content of 0.5–35 wt.%, heating the suspension to a temperature of 116-157 ° C, forcing the heated suspension under pressure to obtain protein fibers, unloading the fibers into the collection zone, followed by the introduction of sodium carbonate to establish a pH of 6 to 7 [3].
    However, protein fibers obtained by a known method cannot be used as additives to meat products and their yield is low.
    The chain of the invention is to increase the yield of fibers used as up to: 15 additives for meat products.
    This goal is achieved in that according to the proposed method for producing protein fibers, which provides for the preparation of an aqueous suspension from a soluble thermal protein-containing raw material having a pH of 4.5-5.0 with a solids content of 0.5-35 wt.%, Heating the suspension to a temperature of 116157 ° C, forcing the heated suspension under pressure to obtain protein fibers, discharging the fibers into the collection zone, followed by the introduction of sodium carbonate until a pH of 6 to reach. 7, the introduction of sodium carbonate into protein fibers is carried out immediately before unloading them into the collection zone by injecting sodium carbonate into the stream of protein fibers.
    The aqueous sodium carbonate solution is preheated.
    The introduction of sodium carbonate into protein fibers provides a modification of their pH, preferably between 6th and 7th, without reducing the yield of protein fibers or changing their functional properties, while ensuring maximum yield of protein fibers from a given weight of the protein suspension, since the pH does not change until fiber formation.
    In FIG. 1 schematically shows a heat exchanger for producing protein fibers; in FIG. 2 - diaphragm with exhaust expander.
    The heat exchanger for producing protein fibers consists of a casing 1 with an inner chamber 2 and inlet and outlet pipes 3 and 4, placed inside the casing of the tubular section 5, a pipe 6 for supplying a protein suspension and a collection zone 7 with a diaphragm 8 to create a limited or back pressure.
    The flow of fibers exiting the diaphragm 8, which creates back pressure into the collection zone 7, is limited by the outlet expander 9, and the latter is also intended for injection of carbonate, an influx of protein fibers until they are installed from 6 to 7.
    In FIG. 2 shows a diaphragm 8 with an outlet expander 9 with a conical diverging cross section with a critically set overall discharge angle between 4 and 90 °, <measured from the theoretical axis .10 passing through the center of the diaphragm 8 (nozzle). This angle provides control of the unloading of fibers and the equalization of the flow of unloaded fibers into the collection zone 7, to obtain the necessary pH uniformity, thereby preventing random unloading of fibers, as well as clumping or accumulation of fibers at the edges of the disputed zone.
    The diaphragm 8 has a hole 11, located mainly at an angle, the magnitude of which depends on the theoretical axis 10 passing through the center of the diaphragm, and the preferred spray angle for the diaphragm holes is 5 °.
    The exhaust expander 9 restricts the flow of the suspension within the total discharge angle between 4 and 90 °, including the angles δ and Θ.
    The total discharge angle (8 + Θ) of the conical expander 9 should be equal to or greater than the angle of discharge of the slurry from the / diaphragm 8. The length of the conical divergent section of the exhaust expander 9 should preferably be approximately 25.4 mm and most preferably the limits of 76.2-304.8 mm ..
    The diameter of the external outlet of the conical expander 9 can be of any size and is not critical for the implementation of the proposed method *
    To introduce an aqueous solution of sodium carbonate into the protein fibers until a pH of 6 to 7 is established, there are nozzles 12 in the expander 9. Injection of the sodium carbonate solution at this point through the nozzles 12 provides the most uniform mixing of the alkaline material with the fibers and provides a stable product with a modified pH .
    Shel, chi, hydroxides of alkaline earth elements and various salts that increase pH, as well as mixtures of these substances, can be used to modify the pH of the fibers.
    The sodium carbonate solution used usually has a concentration of 8 to 13 wt.%, The latter being dependent on the rate at which the solution was pumped through the holes 11,
    The method is as follows.
    An aqueous suspension is prepared from a soluble thermal protein-containing raw material with a solids content of 0.5 0.35 wt.%, Mainly 20-35 wt.%. As a raw material, use your own or other protein materials of oilseed, in particular sesame, cotton, peanuts.
    It is advisable to use sources of animal protein, such as gluten and casein, or microbial protein from. sources such as brewing yeast or corpse, depending on the functional characteristics of the product.
    The pH of the suspension is 4.5-5.0.
    Then the suspension is heated to 116157 ° C by passing through a heat exchanger, the heated suspension is pressed through a diaphragm 8, having one * or several holes with a diameter of 0.38-30 0.76 mm, under pressure from 3.5 to 350 kgf / cm 2 with obtaining protein fiber.
    Next, an aqueous solution of sodium carbonate is introduced into the protein fibers until a pH of 6 to 7 is established by injecting it through the nozzles 12 into a stream of protein fibers immediately before they are discharged into the collection zone 7. Before injection, an aqueous solution of sodium carbonate with a concentration of 8 to 13 wt.% Is heated up to about 121 ° C.
    Example. A protein suspension, comprising 438.8 kg of isolated soy protein with a solids content of 24.0 wt%, is mixed with 11.7 kg of coke oil, and the pH of the suspension is adjusted to 4.7 by adding 50% sodium hydroxide solution.
    The protein suspension is mixed in a colloid mill and sent through a heat exchanger with mowing. 151 ° C. Then the suspension is passed under pressure through a flat diaphragm having 15 holes with a diameter of each—. 0.48 mm. 55
    The exhaust expander 9 is placed above the flat diaphragm, which additionally has four holes with a diameter of 10
    921450 6 rum 0.48 mm, each of which is placed at a distance of 90 ° around the outlet expander for injection of a solution that increases the pH. A solution to about pH po- sheniya representing a 13% -. An aqueous solution of sodium carbonate heated to 121 ° C is injected into the outlet expander. The injection rate of the sodium carbonate solution is adjusted to obtain a pH of about 6.4 for the fibers. ''
    The collected fibers have a pH of 6.4 and have a predetermined structure.
    The proposed method for producing protein fibers can increase the yield of fibers used as additives in the production of a wide variety of food products.
    The resulting protein fibers can serve as additives to meat products, giving them improved aesthetic properties, good taste and better culinary properties.
    In addition, the protein protein obtained reduces the cost of various types of meat products when introduced into them.
    权利要求:
    Claims (3)
    [1]
    (54) METHOD FOR OBTAINING PROTEIN FIBERS The invention relates to a technique for producing protein fibers from protein material used to add meat to meat products in the food industry. A known method for producing a protein food product consists in that. that a suspension of defatted soybeans is prepared, HC is added to pH 4.3, the resulting precipitate is dried, added to the initial precipitate in an amount — the pH value is adjusted to 7% and the mixture is fed into an extruder, the output of which protein fibers have a temperature of 150 ° C. 11. There is also known a method for producing protein fibers, which involves preparing an aqueous suspension from plant material, heating the suspension by passing through a heat exchanger with a solids content of 0.535 wt.%, pressing e heated slurry through the diaphragm under pressure to obtain betisovyh fibers and fibers 1gruzku team zone 2. The formed protein fibers are widely used in the preparation times large oobrazi foodstuff having improved aesthetic properties and taste. However, these known methods do not presuppose adjusting the pH of the suspension prior to the beginning of fiber formation in the desired range from 6.0 to 7.0, as a result of which these fibers cannot be used as a source of supplement. Protein fibers having a pH in the range of from 6.0 to 7.0 have more improved culinary properties when added to mous than those having a lower pH from 4.5 to 5.5. The closest to the proposed technical essence and the achieved result is a method of obtaining protein fibers, involving the preparation of an aqueous suspension of a soluble protein-containing raw material, having a pH of 4.5-5.0 with a solid content of 0.5-35 wt.%, Heating the suspension. to a temperature of 116-157 ° C, selling the heated suspension under pressure to obtain protein fibers, discharging the fibers into the collection zone, followed by the introduction of sodium carbonate to establish a pH of 6 to 7 3. However, the protein fibers produced by the known method can not be enjoyed uc as additives to m waist products and their yield is low. The purpose of the invention is to increase the yield of fibers used as additives to meat products. The goal is achieved by the fact that according to the proposed method of obtaining protein fibers, it is necessary to prepare an aqueous suspension from a solvent protein-containing raw material having a pH of 4.5-5.0 with a solids content of 0.5-35% by weight, heating the suspension to a temperature of 116157 c, pushing the heated suspension under. pressure to produce protein fibers, discharging the fibers into the collection zone, followed by the introduction of sodium carbonate to a pH of 6 to. 7, the introduction of sodium carbonate into protein fibers is carried out directly before being discharged into the collecting zone by injecting sodium carbonate into the protein fiber stream. In this case, the aqueous solution of sodium carbonate is preheated. The introduction of sodium carbonate into protein fibers provides for a modification of their pH, preferably between 6th and 7th without reducing the yield of protein fibers or altering their functional properties, thus ensuring the maximum yield of protein fibers from a given weight of protein suspension, so the pH does not change The point of formation is Volohon. FIG. 1 shows schematically a heat exchanger for obtaining protein fibers; in fig. 2 — a diaphragm with an outlet expander. A heat exchanger for receiving baffles fibers consists of a casing 1 with an internal chamber 2 and an inlet and outlet nozzles 3 and 4 located inside the casing of the tubular section 5, a nozzle 6 for supplying protein suspension and a collecting zone 7 s diaphragm 8 to create a limited or reverse pressure. The flow restriction to the flare coming out of the diaphragm 8, which creates a back pressure in the collecting zone 7, is provided by means of an outlet spreader 9, the latter being also intended to inject sodium carbonate into the flow of 6enkb &amp; bix fibers before setting their pH from 6 to 7. At FIG. Figure 2 shows a diaphragm 8 with a discharge expander with a conical divergent section with a critical unloading angle between 4 and 90 f measured from the theoretical axis of the TO passing through the center of the diaphragm 8 (nozzle). This angle ensures the fiber unloading and alignment of the flow of the discharged fibers into the collecting zone 7, obtaining the necessary pH homogeneity, thus preventing the random discharge of the fibers, as well as the clumping or accumulation of fibers along the edges of the sphere. The diaphragm 8 has an opening 11, which is preferably located at an angle, the magnitude of which is dependent on the theoretical axis 10 passing through the center of the diaphragm, and preferred. the spraying angle for the orifices of the diaphragm is 5. The discharge expander 9 limits the flow of the suspension within a total discharge angle between 4 and 9 °, including corners 5 and c. The total discharge angle (5 + O) of the conical expander 9 should be equal to or greater than the angle of discharge of the suspension from the diaphragm 8. The length of the conical discharge section of the discharge section of the expander 9, preferably, should be equal to, Approximately 25.4 mm and, most preferably, within 76.2-304.8 mm. The diameter of the external outlet of the conical expander 9 can be of any size and is not critical to the implementation of the proposed method. For the introduction into the protein fibers of an aqueous solution of sodium carbonate until the pH is within from 6 dr 7 in the expander 9 there are nozzles 12. Injection of sodium carbonate solution at this point through the nozzles 12 ensures: the most uniform displacement of the alkaline material with the fibers and obtaining a stable product with modified pH. To modify the pH of the fibers, pH, pH, hydroxide salts can be used, as well as emit from these substances. The sodium carbonate solution used usually has a concentration of 8–13 wt.%, The latter depending on the rate at which the pump solution is pumped through the holes 11. The method is carried out as follows. An aqueous suspension is prepared from a solvent-bearing protein-containing raw material with a solids content of 0.5-0.35% by weight, preferably 2O-35 wt. The raw material is your own or other oilseed protein materials, in particular sesame, cotton, peanuts. It is advisable to use animal protein sources, such as gluten and casein, or microbial protein from. sources such as brewing yeast or torula, depending on the functional characteristics of the product. The pH of the suspension is 4.5-5.0. The suspension is then heated to 116157 ° C by passing through a heat exchanger, the heated suspension is forced through a diaphragm 8, having one or more holes with a diameter of 0.38 0.76 mm, under pressure from 3.5 to 350 kgf / cm to produce protein fibers. Next, a sodium carbonate solution is added to the protein fibers to establish a pH in the range of 6 to 7 by injecting it through the nozzles 12c of the protein fiber stream just prior to their discharge into the collecting zone 7. Before injection, an aqueous solution of sodium carbonate with a concentration of 8 to 13 wt. % heat up to about 121 g. Example. The protein suspension, containing 438.8 kg of isolated soy protein with a solids content of 24.0 wt.%, Is mixed with 11.7 kg of coke oil, and the pH of the suspension is adjusted to 4.7 with 50% sodium hydroxide solution. ..,; The protein suspension is stirred in a colloid mill and sent with the aid of sa through a heat exchanger at 151 ° C. Then the suspension is passed through the pressure through a flat diaphragm having 15 holes with a diameter of 0.48 mm each. The outlet expander 9 is placed above the flat diaphragm, which additionally has four diaphragm holes at a distance of 90 around the outlet expander to inject the solution that raises the pH. The pH solution, which is a 13% aqueous solution of sodium carbonate heated to 121 ° C, is injected into the outlet expander. The rate of injection of sodium carbonate solution is adjusted so as to obtain a pH of about 6.4 for the fibers. The collected fibers have a pH of 6.4 and have the desired structure. The proposed method for producing protein fibers allows an increase in the yield of fibers used as additives in the production of a wide variety of food products. The resulting protein fibers can serve as additives to meat products, giving them improved aesthetic properties, good taste and better culinary properties. In addition, the resulting protein fiber reduces the cost of distinction 1L) 1X types of meat products when it is introduced into them. Claim 1, a method for producing protein fibers, comprising preparing an aqueous suspension from a solvent protein solution of a raw material having a pH of 4.55, 0 and containing 0.5-35% by weight of solid hanging, heating the suspension to 116157 ° C, pressing the heated suspension under pressure to produce protein fibers, fiber loading into the team zone, followed by the introduction of sodium carbonate to a pH of 6 to 7, different from the fact that, in order to increase the flow of fibers used as additives to meat products, the maintenance of sodium carbonate The protein fibers were directly transferred to the collection zone by the injection of sodium carbonate into the outflow of protein fibers. 2. The method according to claim l, is different from the fact that the aqueous solution of sodium carbonate is preheated. Sources of information taken into account in the examination. Japan patent number 5O-2O24, l. And 23 J 3/00, pubpick. 1975.
    [2]
    2. US patent number 3662672, l. 99-17, published. 1972.
    [3]
    3.UK patent number 14О43О5, l. D 1 1. publish. 1975.
    g /
     jIT - |
    7:% r
    类似技术:
    公开号 | 公开日 | 专利标题
    CA1172091A|1984-08-07|Process for cooking or gelatinizing materials andproducts
    SU921450A3|1982-04-15|Method of producing protein fibres
    EP0438783B1|1996-03-20|Method and apparatus for cooking and spray-drying starch
    DK2091338T3|2019-03-04|Process for continuous preparation of a porous powdered product
    US4125635A|1978-11-14|Method for making a meat analog
    US4350713A|1982-09-21|Production of sponge cake
    CA1087448A|1980-10-14|Continuous gelatinization process
    US4410554A|1983-10-18|Soy protein product and process
    EP0103015A1|1984-03-21|Method for preparing cooked wheat product.
    US3852503A|1974-12-03|Method of making puddings containing soy protein
    US4438681A|1984-03-27|Installation for solubilizing cocoa
    US4346652A|1982-08-31|Apparatus for making a meat analog
    US2324951A|1943-07-20|Foam stabilizing composition
    US3210195A|1965-10-05|Preparation of spun protein food products
    US3928641A|1975-12-23|Method of collecting protein filaments
    US4062987A|1977-12-13|Protein texturization by centrifugal spinning
    US4038431A|1977-07-26|Protein texturization by steam injection
    US4490397A|1984-12-25|Process for the production of protein fibres
    US3038809A|1962-06-12|Process for producing starch jellies
    US4168657A|1979-09-25|Protein texturization by steam injection
    US4226576A|1980-10-07|Protein texturization by centrifugal spinning
    US3493386A|1970-02-03|Puffed fibrous food product and process of preparing same
    US2891045A|1959-06-16|Method of drying gluten
    Hartman1978|Texturization through spinning
    GB779374A|1957-07-17|A method and apparatus for continuous production of yeast dough
    同族专利:
    公开号 | 公开日
    NO764205L|1977-06-14|
    NL162436C|1980-05-16|
    FI763204A|1978-05-10|
    SE7613939L|1977-06-12|
    FI58713B|1980-12-31|
    DE2655747B2|1979-01-04|
    SE423025B|1982-04-13|
    NO143395B|1980-10-27|
    GB1550878A|1979-08-22|
    NL162436B|1979-12-17|
    FI58713C|1981-04-10|
    JPS5272854A|1977-06-17|
    US4017646A|1977-04-12|
    FR2334305A1|1977-07-08|
    ES453783A1|1978-01-16|
    DE2655747C3|1979-08-30|
    YU298076A|1982-05-31|
    CA1067337A|1979-12-04|
    NL7613739A|1977-06-14|
    NO143395C|1981-02-04|
    JPS605256B2|1985-02-09|
    DE2655747A1|1977-06-23|
    PL101457B1|1978-12-30|
    引用文献:
    公开号 | 申请日 | 公开日 | 申请人 | 专利标题
    US3821453A|1969-05-19|1974-06-28|Ralston Purina Co|Protein fiber forming|
    US3662672A|1969-05-19|1972-05-16|Ralston Purina Co|Protein fiber forming|
    US3662671A|1969-05-19|1972-05-16|Ralston Purina Co|Protein fiber forming|
    US3800053A|1972-06-26|1974-03-26|Gen Mills Inc|Process for preparing protein monofilaments|
    US3928641A|1974-10-29|1975-12-23|Ralston Purina Co|Method of collecting protein filaments|JPS5913172B2|1977-09-10|1984-03-28|Fuji Oil Co Ltd|
    US4321280A|1977-12-01|1982-03-23|General Foods Corporation|Textured oil seed protein products|
    US4234609A|1978-08-28|1980-11-18|Ralston Purina Company|Method of forming food product from mollusks and product thereof|
    JPS6210627B2|1980-09-22|1987-03-07|Fuji Oil Co Ltd|
    JPS6228656B2|1980-09-22|1987-06-22|Fuji Oil Co Ltd|
    US4360653A|1981-10-23|1982-11-23|Ppg Industries, Inc.|Polymerizate ofand aliphatic polyurethane having acrylic unsaturation|
    US4551351A|1984-02-09|1985-11-05|Fuji Oil Company, Limited|Process for producing meat block-like protein material|
    US11019836B2|2015-08-03|2021-06-01|Savage River, Inc.|Food products comprising cell wall material|
    法律状态:
    优先权:
    申请号 | 申请日 | 专利标题
    US05/639,721|US4017646A|1975-12-11|1975-12-11|Process for producing pH modified protein filaments|
    [返回顶部]