• 专利附录
  • 专利说明
  • 权利要求
  • 类似技术
  • 同族专利
  • 引用文献
  • 法律状态
  • 优先权
    • 专利摘要:
    The invention relates to a method for removing residues from a gasifier, a device for carrying it out and reducing the duration of the process. The method includes the steps of granulating the residues in a water bath, draining the heated water mixture fi residues using a water containing sluice, supplying water to the water bath and the sluice, equalizing the pressure between the sluice and gasifier from the water bath and reducing the sluice pressure. A distinctive feature of the method is that the heated mixture of water and residues is first separated in the chamber connected to the sluice to the water recirculated to the water bath and the residues supplied to the water filled pshyuz and before the pressure in the gateway and the separation chamber conducted at one time, the heated water in the chamber is cooled or replaced with cold water, the water being fed to the sluice through a separation chamber. A device for carrying out the method comprises a water bath located in the lower part of the gasifier, connected to the gateway through a pipeline with shut-off members located therein and provided with a water supply pipeline entering the lower part, the tank to be supplied to the gateway located above the gateway and at a distance from it and provided with a pipeline located in the lower part about a shut-off element placed in it, and a container for receiving solid residues connected to the lower part of the gateway through a pipeline placed in m locking body. A distinctive feature of the device is that the gateway is connected to a separating chamber located above it, the upper part of which is provided with an annular pipeline connected to the pipeline located in the lower part of the tank for supplying water to the gateway, with the pipeline for supplying water to the lower part of the gasifier with the locking member located therein entering the tank for receiving solid residues, and with the pipeline with the locking member accommodated therein, the inlet is at the top of the tank for supplying water to Gateway. 2 sec. f-ly, 2 3.p. f-ly, 3 ill. SO with so se: about 00 s
    公开号:SU1301318A3
    申请号:SU833625854
    申请日:1983-08-01
    公开日:1987-03-30
    发明作者:Гиббель Иозеф；Герхардус Ульрих；Шмидт Фолькмар；Лидер Бернхард；Шеве Гейнрих；Церрес Эрвин
    申请人:Рурхеми Аг (Фирма)；
    IPC主号:
    专利说明:

    eleven
    The invention relates to the removal of residues, in particular, to a method for removing residues from a gasifier, as well as a device for carrying it out.
    The aim of the invention is to accelerate the process of removing residues from the gasifier.
    Fig, 1 shows the device, a general view; in fig. 2 - separation chamber; in fig. 3 - guide element of conical shape.
    A device for carrying out the method includes a water bath 1 located in the lower part of the gasifier. The water to the bath 1 is connected to the gateway 2 located under it by means of the pipeline 3 with shut-off members (valves) 4 and 5 and a flexible connection, for example a compensator 6. The water to the bath 1 is provided with a pipeline 7 for supplying water to it . Gateway 2 is connected to a tank 8 for supplying water to it via a pipe 9 with a shut-off element 10 placed on it. A tank 13 for receiving solid residues is connected to the lower part of the gateway 2 by a pipe 11 with a shut-off organ (valve) 12 placed on it. A separating chamber 14 is installed above the gateway 2, the upper part of which is provided with an annular conduit 15 connected to conduits 9 and 7 and to a conduit 16 having a shut-off member I7 and connecting the annular conduit 15 to a reservoir 13. The annular conduit 15 is connected to the upper part of the reservoir 8 for supplying water to the sluice 2 by means of a pipeline 18 with a shut-off element 19. The separating chamber 14 is provided with a central nozzle 20 and guiding elements 21 arranged parallel to each other, forming the central channel 22, the bottom st distribution which is put on top of the gateway 2. The guide gatsie elements 21 may be formed as conical or inclined plates.
    The gasification residues formed in the gasifier at 10–200 bar and 1100–1700 ° C enter the water bath 1, are cooled there, granulated in water and, as a suspension, pass through the open stop valve 4, the compensator 6, the open stop valve 5 into the separation valve chamber 14 connected to gateway 2 and under the same high pressure as 182
    the second is in the gasifier. The separation chamber 14 is provided with a level gauge 23. The 1Cluse 2 has two level gauges 24 and 25, as well as a pressure gauge 26 and is cooled by a jacket 27.
    The water in the bath 1 has a temperature dependent on the partial pressure of water vapor in the synthesis gas, for example 200 C. In order to avoid an unacceptable increase in the concentration of dissolved salts and fine-grained solids in the water, through a pipe 28, the amount of circulating water or fresh water. The controller 30 maintains a constant water level in the bath 1 by turning on the throttle organ (valve) 31 in the discharge pipe 32 containing the coolers 33 and 34. The granulated residues with poor sedimentation capacity are removed from the water bath 1 into the separation chamber 14 by a feed unit, for example a pump 35, connected via pipe 36, ring pipe 15 and valve 37 with a separation chamber 14. In this chamber, hot water is separated from slag. The water discharged from the separation chamber is recycled together with the circulating water through conduit 7 to the water bath 1.
    Due to the suction effect of the pump 35, the mixture of water and slag enters through the nozzle 20 into the separating chamber 14. The velocity of the mixture and slag in the feed channel is higher than between parallelly located directions l and upwards the surfaces of the guide elements 21. 21, there is a slower flow rate and sedimentation of solids. Larger slag particles fall during this loading through the nozzle 20 into the station 1c under the separation chamber I4 gateway 2.
    Since the separation chamber 14 and the sluice 2 connected to it are always completely filled with water, the cold content of the sluice 2 is not mixed with the mixture of hot water and slag entering the chamber 14. Hot water is directed into chamber 14 along the conical direction of element 21 and is recirculated into the water bath 1 via an annular
    313
    pipeline 15 entering pipe 36 through valve 37, pump 35. valve 38 and pipeline 7.
    After loading the sluice 2 with slag, the valves 29 and 31 are closed simultaneously. The supply of water through line 28 and the discharge of water to line 32 is stopped. Due to the closing of the valve 4, the connection with the water bath 1 is stopped, and the recirculation of water from the separation chamber 14 to the water bath 1 is stopped by closing the valve 38. As a result of opening the valve 39, the hot water in the separation chamber 14 is cooled the cooler 40 located in the pipe 41 connecting the separating chamber 14 and the ring pipe 15 to the suction pipe 36 of the pump 35 through the pipe 3. After cooling the hot water, the pressure can be reduced.
    The displacement of hot water under pressure in the separation chamber 14 by the addition of cold water is possible. For this purpose, cold water is added to the separation chamber 14 from the pipe 28 through the pipe 42 connecting the pipe 28 through the valve 43 to the pipe 3. At the same time, the hot water in the separation chamber 14 is discharged through the ring pipe 15, the pipe 32, cooler 33 and valve 31, which is open to the appropriate value. Valves 37 and 39 are closed. After displacing the hot water and closing the valve 31, it is possible to lower the pressure in the separation chamber 14 and gateway 2.
    In addition, hot water under pressure in the separation chamber may be expelled into water vapor by the addition of cold water. In this case, cold water is supplied in the manner described above, i.e. through conduit 28, conduit 42, valve 43 and conduit 3. The displaced hot water leaves the separation chamber 14 through the annular conduit 15, conduit 36, the valve 37 which opens, the pump 35, the valve 38, which also opens, and enters through the pipe 7 into the water bath 1. After displacing the contents of the separation chamber 14, the valves 43 and 37 are closed. Then in the separation chamber 14 and the gateway 2 can reduce the pressure. By-
    184
    The pressure in the separation chamber 4 and the sluice 2 is reduced through an annular pipe 7, a pipe 18, which by opening the valve 19 with valves 37 and 39 simultaneously closed, connects the separation chamber with a capacity of 8, which is under a pressure of 0.05-4 bar and equipped with a pipe 44 for the removal of waste gases. This releases gaseous substances dissolved in water (CO and H).
    Pressure equalization takes place spontaneously. The valve 19 is then closed. The pressure is reduced to atmospheric pressure by means of a receiving tank 13 by opening the valve 17, through a pipe 16, which is also connected to the ring pipe 15. The receiving tank 13 is provided with a mechanical means 45 for separating slag and water.
    A residual amount of gas that is under reduced pressure is sucked off through conduit 46 and is fed for processing, for example, by incineration.
    Unloading separation chamber
    14 and the gateway 2 connected to it is performed by opening the valve 10 located in the connecting pipe 9 between the tank 8 and the pipe 36, and opening the valve 12 located in the connecting pipe between the gateway 2 and the receiving tank 13. From the tank 8, the water now flows through the annular pipeline
    15c separating chamber 14 and washes out the slag, which is located between the individual conical parallel guiding elements 21, to gateway 2. The mixture of water and slag flows through the open valve 12 into the receiving tank 13, where water and slag are separated.
    From the receiving tank 13, water enters the tank 8 through the pump 47 and regulates the 1st valve 48 valve 49. Water lost in the tank 13 due to the separation of water and slag is compensated through the pipe 50 with the POM1TSI located on the tank 8 of the level gauge 51, opening a valve 53 located on line 52. Thus, a predetermined level of liquid is provided in the tank 8.
    Full unloading of the tank 13 is carried out due to premature
    closing the valves 10, 12 and 17. Thus, the gateway 2 and the separation chamber 14 are always filled with water. Then slag can be fed back to gateway 2
    Pressure equalization between bath 1 and gateway 2 is accomplished by opening valve 54 in line 55 connecting pipe 36 to pipe 7. Pressure gauge 56 shows pressure equalization. Since the connecting pipes 3, 36 and 28 and the separation chamber 14 are completely filled with water, the pressure between the water bath 1 and the separation chamber 14 is equalized spontaneously through the aqueous medium. As a result of closing the valves 54 and 39 and opening of the locking bodies 4, 37 and 38, the water bath is connected to the distributor 20 via a pipeline with a dividing chamber, and the slag from the water bath 1 is again charged to the separating chamber. and 31 controller 30 is activated again.
    shut-off valve on it, characterized in that, in order to speed up the process, it is provided with a separation chamber connected
    25 with the gateway and located above it, the upper part of the separation chamber is provided with an annular pipe connected to the pipe located at the bottom of the tank for
    权利要求:
    Claims (4)
    [1]
    1. A method of removing residues from a gasifier, including supplying water to a gasifier water bath, supplying water to a lock from a tank, granulating residues in a water bath, draining water and residues to a lock, equalizing the pressure between the lock and the gasifier, reducing the pressure in the lock by connecting it to a water supply tank and removing residues from a sluice, characterized in that, in order to accelerate the process, the heated mixture of water and residues is fed to a separation chamber connected to the sluice, and separated into water and a residue entering the sluice, at Pressure equalization between the gateway and the gasifier is carried out by supplying water from the separation chamber to the water bath, before the pressure in the gateway is lowered, the heated water in the separation chamber is cooled or replaced with cold water and pressure reduction in the gateway is carried out by connecting the separation chamber to the dp supply tank water and water in the gateway lead through the separation chamber.
    [2]
    2. A device for removing residues from the gasifier, comprising a water bath located in the lower part of the gasifier, connected to the gateway located under it by means of a pipeline placed on
    locking bodies, a pipeline for supplying water to a water bath, located in its lower part, a container for supplying water to a lock, located above the lock and at a distance
    from it and equipped with a pipe located at the bottom with a stop valve placed on it, and a container for receiving solid residues connected to the bottom of the gateway
    through the pipeline with
    shut-off valve on it, characterized in that, in order to speed up the process, it is provided with a separation chamber connected
    with the gateway and located above it, the upper part of the separation chamber is provided with an annular pipe connected to the pipe located at the bottom of the tank for
    supplying water to the sluice, with a pipeline for supplying water to the lower part of the water bath, with a pipeline with a stop valve placed in it, which is included in the container for receiving solid
    residues, and with a pipeline with a shut-off valve placed in it, entering the upper part of the tank, water supply to the sluice, the separation chamber is provided with a central nozzle and guiding elements parallel to each other, forming a central channel, the lower part of which is located in the upper part of the sluice .
    45
    50
    [3]
    3. The device according to claim 2, characterized in that the guiding elements are made in the form of a cone.
    [4]
    4. The device according to claim 1, about tl and - the fact that the guide elements are made in the form of inclined plates.
    P
    figure 1
    /five
    FIG. 2
    cpt / e. J
    Compiled by N. Ageeiko Editor L. Veselovska Tehred. Kadar JCoppeKTOp I. Muska
    Order 1163 / 58Tierah 464Subscription
    VNIIPI USSR State Committee
    for inventions and discoveries 113035, Moscow, Zh-35, Raushsk nab., 4/5
    Production and printing company, Uzhgorod, st. Project, 4
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    引用文献:
    公开号 | 申请日 | 公开日 | 申请人 | 专利标题
    US3235313A|1964-05-18|1966-02-15|Koppers Co Inc|Sluicing solid materials from spaces under superatmospheric pressure|
    CH563180A5|1973-09-13|1975-06-30|Escher Wyss Ag|
    DE2444819B2|1974-09-19|1980-01-03|Steag Ag, 4300 Essen|Process for cleaning the gas produced in the gasification process|
    DE2455127C2|1974-11-21|1986-02-27|Shell Internationale Research Maatschappij B.V., Den Haag|Process for discharging residues from a gasification chamber under increased pressure|
    FR2417326B1|1978-02-15|1980-08-29|Tepral Grpt Interet Economique|
    DE2815329A1|1978-04-08|1979-10-18|Ruhrkohle Ag|METHOD FOR THE TREATMENT OF WATER / CARBON SUSPENSIONS WHICH ARE INCLUDED WHEN WASHING OUT THE GAS RESULTING FROM THE GASIFICATION OF MINERAL RAW MATERIALS|
    DE2829629C2|1978-07-06|1982-07-29|Ruhrchemie Ag, 4200 Oberhausen|Method and device for discharging residues from the pressure system of a pressure gasification plant|
    US4342638A|1979-04-02|1982-08-03|Envirotech Corporation|Flashed-down residue treatment including filtering and solvent repulping|
    BR8105270A|1980-11-12|1982-08-31|Texaco Development Corp|PROCESS FOR THE PRODUCTION OF SYNTHESIS GAS SUBSTANTIALLY FREE OF PARTICLES|
    US4459134A|1982-09-15|1984-07-10|Texaco Inc.|Outlet structure for a downflow generator|US4533363A|1984-01-20|1985-08-06|Texaco Development Corporation|Production of synthesis gas|
    US4852997A|1987-10-05|1989-08-01|Shell Oil Company|Slag water bath process|
    US20020043023A1|1994-06-27|2002-04-18|William M. Davis, Jr.|Slag handling system|
    DE10118443A1|2001-04-12|2002-10-17|Bokela Ing Gmbh|Material separation comprises feeding material mixture in flow direction running parallel to gravitational field through channel, and conveying scrubbing liquid|
    US20070210012A1|2006-03-09|2007-09-13|Energy & Environmental Research Center Foundation|Wet solids removal and separation system|
    DE102006040077C5|2006-08-28|2014-06-05|Siemens Aktiengesellschaft|Apparatus for discharging slag from gasification reactors|
    US20080115479A1|2006-11-17|2008-05-22|Mitsubishi Heavy Industries, Ltd.|Pressurized coal gasifier and coal gasification combined cycle power plant|
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    JP5484850B2|2009-09-30|2014-05-07|三菱重工業株式会社|Slag discharge system|
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    法律状态:
    优先权:
    申请号 | 申请日 | 专利标题
    DE19823230088|DE3230088A1|1982-08-13|1982-08-13|METHOD AND DEVICE FOR DISCHARGING RESIDUES OF ASH-FUELING FUELS|
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