• 专利附录
  • 专利说明
  • 权利要求
  • 类似技术
  • 同族专利
  • 引用文献
  • 法律状态
  • 优先权
    • 专利摘要:
    the present invention describes the preparation method and the integrated nutritional powder, the raw material of this integrated nutritional powder is comprised of the presence of: vitamin b1, vitamin b2, vitamin b6, pantothenic acid, nicotinic acid, vitamin b12, vitamin c, vitamin a, vitamin k, vitamin d, vitamin e, biotin, folic acid, calcium, magnesium, iron, zinc, selenium, chromium, copper, manganese, corn fiber powder, inulin, soy protein isolate powder, husk extract black bean extract, agaricus mushroom extract, soy lecithin, red bean extract, l-carnitine, ß-carotene, lycopene, citrus extract, vanadium, acerola extract, grape seed extract, maltodextrin, essence, aspartame, and acesulfame potassium. This integrated nutritional powder is a kind of food that is in directional development in order to work together with low carb diets and the amount of regular exercise, specially formulated to address obesity and level three fitness program, not only achieving weight loss, as well as significant level three rehabilitation effect, facilitating wide-area popularization.
    公开号:BR112016016588B1
    申请号:R112016016588-8
    申请日:2014-08-18
    公开日:2021-09-14
    发明作者:Lu Mingfu；Zhang Xiuping
    申请人:Lu Mingfu；
    IPC主号:
    专利说明:

    FIELD OF INVENTION
    [0001] The present invention belongs to the field of nutritional food which refers to a method of preparing integrated nutritional powder, more specifically, this invention concerns a nutritional intervention for lifestyle diseases (mainly such as obesity, hypertension, high blood sugar, high cholesterol levels). FUNDAMENTALS OF THE INVENTION
    [0002] Currently there are many nutritional supplement products on the international market of which most are used as daily nutritional supplement for everyday people; a part of these products is for the nutritional fortification of specific groups such as children, pregnant women, the elderly, etc. Integrated nutrition for weight loss already exists, like Herbal Life and Shaklee (USA), and Sunny Healthy (Japan). But these products usually have limitation of their formula, not being suitable for the obesity of Chinese people.
    [0003] Chinese published patent document CN101637255A discloses a nutritional powder that can effectively lower blood sugar and lower urine sugar consisting of the following raw materials with their respective weights: Wheat bran: 5-25 parts, wheat saracen: 5-20 parts; oats: 5-20 parts; white corn: 5-20 pieces; Chinese beans: 5-15 pieces; panicum miliaceum (millet): 5-15 parts, red beans: 3-10, peas: 3-10 parts; sorghum: 3-10 parts; sesame: 2-10 parts; tremella fuciformis (gelatinous fungus): 1-5 parts; lily: 1-5 parts; goji 1-5 parts. Method: every 10 parts of wheat bran add 1-2 part vinegar and mix well 0.5-1 part sugar; add water for cornbread consistency; cook for 20-30 min; cool, dry and grate; bake until yellow surface and break until reaching a fineness of 100-200 powder; wash the sesame, dry, fry and crush to a fineness of 60-80 powder; wash the goji, lily and tremella fuciformis (gelatinous fungus), dry and grind them to a fineness of 60-100 powder; after grinding all raw material, mixing and packaging. It is a diet therapy for those suffering from diabetes and high cholesterol, or as a raw material for a basic food or food supplement, from auxiliary therapy. However, this product ends up being poor, as it has a therapeutic basis.
    [0004] Chinese patent document CN102273520B teaches a method of preparing nutritional powder of a type of whey. This nutritional powder generates liquid whey and uses chickpeas as a raw material for the production of fermented cheese, combined with scientific nutritional needs, through a refining process to regulate blood fat. This nutritional powder is rich in nutrients that the body digests and natural protein that the body absorbs. Among the 18 amino acids, nine types of amino acids are essential (including histidine which is required for children), the proportion is 40% of the total amino acids; the content of unsaturated fatty acids is 61%; the lactose content is 5.58%, and the powder is rich in Vitamin B2, Vitamin C and other vitamins and high levels of potassium, calcium, magnesium, zinc, iron and other minerals. The Document states that this nutritional powder is conducive to physical fitness, is a nutritional tonifier and boosts immunity, with essential nutrients in high consumption for children, the elderly, patients with high cholesterol and patients with high blood sugar, a good product nutritional with natural low starch. However, the formula used in the method described is not reasonable, based on nutrition, being inadequate for those with high blood sugar and high cholesterol.
    [0005] Published Chinese patent document CN1146305A discloses a nutritional powder for diabetics that consists of the following elements in its composition: pumpkin powder: 20-40, Chinese bean bran: 20-40, brewer's yeast: 5- 15, wheat flour: 20-40, pectin, 15-30. The document states that this type of nutritional powder can reduce the patient's unbearable hunger due to dietary therapy, thus enabling the patient to execute a dietary treatment plan. The invention is mainly made up of natural foods, so there are no side effects; the cost is low and it is conducive to long-term use by people with different types of diabetes, at the same time, the present invention lowers blood sugar, has a complication-preventing function, thus improving insulin sensitivity, improving insulin sensitivity. effectiveness and reducing the amount of insulin. However, this formula has a distinct lack of directional for those with high cholesterol and high blood sugar. SUMMARY OF THE INVENTION
    [0006] The nutritional powder of the invention is a kind of product effective for lifestyle diseases (mainly obesity, hypertension, high blood sugar, high cholesterol levels) leading to an integrated nutritional powder preparation method of food intervention. DETAILED DESCRIPTION OF THE INVENTION
    [0007] In order to solve the above mentioned prior art problems, the present inventors have intensively studied and proposed the following solutions:
    [0008] In one aspect, the present invention provides an integrated nutritional powder which is composed of the following components: vitamin B1, vitamin B2, vitamin B6, pantothenic acid, nicotinic acid, vitamin B12, vitamin C, vitamin A, vitamin K, vitamin D, vitamin E, biotin, folic acid, calcium, magnesium, iron, zinc, selenium, chromium, copper, manganese, corn fiber powder, inulin, isolated soy protein powder, black bean husk extract, extract from Agaricus mushroom, soy lecithin, red bean extract, L-carnitine, β-carotene, lycopene, citrus extract, vanadium, acerola extract, grape seed extract, maltodextrin, essence, aspartame, ethyl maltol and acesulfame potassium .
    [0009] The preferred weight proportion of each component integrated in the nutritional powder is as follows:


    [00010] As is generally understood in this field, the weight ratio is on a parts-by-weight basis.
    [00011] The formulation of the present invention, for lifestyle diseases (such as obesity, high blood pressure, high blood sugar, high cholesterol) has great nutritional directional interventions.
    [00012] The inventor selected components from a very complex amount in order to obtain the above specific formulation, making the mixture between the compositions can play the role of good compatibility and synergistic effect.
    [00013] Studies have found that vitamin C can be very effective in improving the stability of grape seed extract and Agaricus mushroom extract in the presence of corn fiber powder can further enhance the blood fat reducing effect. This role of compatibility was not reported in previous documents, nor was it simply imagined by the specialist in this area. The formulation of the present invention is the first report with the greatest substantive difference from the whole nutritional powder currently marketed.
    [00014] Preferably, the Agaricus mushroom extract should contain 80% by weight of polysaccharide, which has above 80% by weight of protein binding. The preferred polysaccharide is the one with protein binding (1^6)-β-D-glucan - complex protein element. The present inventors have surprisingly found that protein-bound polysaccharide is better absorbed by the body, thus better utilizing the effect of polysaccharides. In the prior art, it was generally believed that the protein-binding polysaccharide could affect the function of the polysaccharide by removing the protein through the protein removing agent Savage. The present inventors speculated that perhaps in other components of the integrated nutritional powder of the present invention, especially in trace metal elements, the protein-binding polysaccharide could more effectively disaggregate.
    [00015] Preferably the acerola extract should have 5-15% by weight where the 5-hydroxymethyl-furan-2-carbaldehyde is preferably 10% by weight and 50-70% by weight of proline with preferably 60% by weight.
    [00016] Preferably the grape seed extract should have at least 35% by weight, preferably at least 60% by weight, more preferably at least 80% by weight of oligomeric proanthocyanidins.
    [00017] In another aspect, the present invention provides a method for preparing the integrated nutritional powder that includes the steps below:
    [00018] (1). Mix and cut enough for grinding vitamin 81, vitamin B2, vitamin B6, pantothenic acid, nicotinic acid, vitamin B12, vitamin C, vitamin A, vitamin K, vitamin D, vitamin E, biotin, folic acid, vanadium, calcium, magnesium, iron, zinc, selenium, chromium, copper and their inorganic manganese salts in the shear mixer according to the weight of each; the powder particle size must be less than 10μm for the first mix;
    [00019] (2). The isolated soy protein powder and inulin must be mixed evenly in the blender for the second mixture;
    [00020] (3). Corn fiber powder, black bean husk extract, Agaricus mushroom extract, soy lecithin, red bean extract, L-carnitine, β-carotene, lycopene, citrus extract, acerola extract, grape seed extract , maltodextrin, essence, aspartame, ethyl maltol and potassium acesulfame must be mixed together for the third mixture, where it is added to the ethanol and acetone mixture, stirring well until obtaining a liquid mixture, then passed through a spray drying process or lyophilization to obtain a powdered product;
    [00021] (4). The first mix, second mix and said powdered product are added in a mixer for 15-30 min, passed through a 50-80 mesh sieve, sterilized in microwave for 30-60min, packaged and then inspected, thus the product final (integrated nutritional powder) will be complete.
    [00022] In the method of preparing the integrated nutritional powder of this invention, there is no preparation technique, all ingredients are mixed during mixing. This is because the present inventors have discovered that, in one aspect, if there is milling of the extract, perhaps the high temperature caused by the milling work will result in the disintegration of the extract.
    [00023] In another aspect, during the adhesion of the extract, this is easily bound in large proportion to the isolated soy protein powder, resulting in the difficulty of mixing the nutritional powder. The present inventors have found that corn fiber powder and inulin compared to soy protein isolate powder hardly cause strong extract adhesion, so the extract is first mixed with corn fiber powder by spray drying or freeze drying to result in a powdered product. Through this process, the extract is effectively dispersed in the corn fiber powder, again through the good dispersion of the corn powder and completely into the nutritional powder. Another spray drying and cooling is used to lower the temperature in order to prevent the extract from disintegrating.
    [00024] Preferably, in step (3), the weight ratio of the mixture with ethanol is 1:3-1:10.
    [00025] Preferably, in step (3), the volume ratio of ethanol to acetone is 10:1-10:3.
    [00026] In addition, preferentially for the extraction of the Agaricus mushroom extract is adopted the fermentation process. The specific extraction method is as follows: (1) After the Agaricus mushroom has dried, it is ground and passed through a 40 mesh sieve; (2) Fermentation of the Agaricus mushroom: a. Cultivation stock oblique plane: PDA cultivation base; B. Fermentation medium: 3% by weight cornstarch powder, 2% by weight sucrose, 0.15% by weight yeast extract, 0.13% by weight KH2PO4, 0.10% by weight MgSO4. 7H2O, 1mg/100ml Vitamin B1; pH is 5-8; ç. Mycelium cultivation: mixture 1 in a triangular Erlenmeyer flask with 250mL, containing 50mL of liquid and inoculated with 0.15cm2 of bacteria, mixture 2 in a triangular Erlenmeyer flask with 250mL, liquid volume of 50mL, displacing 10% of the bacteria in a liquid medium, placing the same on a rotary shaker and cultivating them for 5-9 days at a temperature of 26°C. (3) After fermentation, the mycelium is washed with distilled water, dried at 50-70 °C and after being ground it is passed through a 40 mesh sieve; (4)For the mycelium passed through the mesh sieve it is necessary to add water, and the weight ratio of mycelium and water is 1:10-1:40, preferably 1:30, the extraction temperature is 70-100 °C, preferably 100 °C, extraction time is 1-6 hours, preferably 5 hours; after the liquid extract is passed through a centrifuge, extract the serum, add 95% ethanol between 3-6 times the volume of serum, centrifuge again to remove the serum until it reaches sedimentation, and then the polysaccharide rich extract is obtained.
    [00027] In the present invention, through fermentation and extraction, it is possible to extract with a higher degree of purity, even reaching about 100% of polysaccharides. Furthermore, as described above, in the prior art no protein removal reagent is used to ensure extraction of a polysaccharide component above 80% by weight, preferably 100% by weight of the protein binding polysaccharides so as to be able to have the greatest degree possible of the complex (1 ^ 6) -β-D-glucan- protein, and thus improve the absorption of polysaccharides.
    [00028] The integrated nutritional powder of this invention promotes energy conversion as well as prevents bodily harm and becomes effective. Details are as follows below: I. Promoting energy for transformation
    [00029] 1. The integrated powder provides enough coenzyme for the "burning" of fat (fat consumption). This process requires a large amount of vitamins and mineral synergy action, and with carbohydrate in daily nutritional balance, the cellular energy situation is different. Furthermore, this new nutritional balance described in nutrition documents remains to be systematically discussed.
    [00030] The inventor has based a large number of practices and in-depth research for new and different formula of daily dietary supplement, achieving a harmonious realization of fat conversion, preventing in various types of research to find a resulting acidic disposition because of incomplete metabolism, as well as preventing acid poisoning problems. At the same time it prevents the appearance of muscle pain, whole body weakness, hair loss, mouth ulcers, bleeding gums, bad breath, constipation and other problems.
    [00031] 2. The integrated nutritional powder of this invention can increase cell activity and accelerate cell regeneration and tissue repair. This process not only requires high-quality raw materials (mainly isolated soy protein), but additional special food acceleration of the natural activity is also necessary; in this context, the formula will be achieved through the addition of the Agaricus mushroom.
    [00032] 3. Deep cleaning of the sedimented fat in the walls of blood vessels and liver is accomplished by adding soy lecithin.
    [00033] 4. Red bean extract is added to strengthen spleen function and improve nutrient use efficiency.
    [00034] 5. For blood glucose and blood pressure problems, supplement the fortification formula with calcium, magnesium, chromium and water-soluble cellulose (inulin).
    [00035] 6. For intractable obesity and severe metabolic disorder, in order to take into account the decreased capacity of L-carnitine (vitamin BT, essential vector of fat cells) of the liver composition, L-carnitine is added in the formula.0 II. Avoid physical damage
    [00036] 1. Low carbohydrate diet limits sugar (especially in main food restrictions) as well as limits cellulose intake, often causing constipation. In the formula, insoluble fiber (corn fiber) is added, solving the problem of dry feces, liquid feces, sticky feces, with bad smell, etc.
    [00037] 2. Accelerated fat burning increases free radicals (which account for 90% of all radicals in the body) in cellular mitochondria. These free radicals can easily damage the inner mitochondrial membrane and mitochondrial genetic material, and cause a variety of chronic diseases. In the formula are added β-carotene, vitamin C, vitamin E, mineral selenium, acerola extract, citrus extract, lycopene, grape seed extract to increase the content of a variety of minerals that improve the system's capacity. endogenous human antioxidant, preventing various types of cell damage caused by free radicals.
    [00038] 3. In the process of energy conversion of the large amount of "garbage" (ie metabolite), the detoxification burden of the kidney and liver increases. By increasing black bean husk extract (for liver and kidney function) in the formula, kidney and liver care are deepened, effectively avoiding paleness problems during the recurrent weight loss process of similar techniques.
    [00039] 4. Burning fat can lead to the consumption of large amounts of minerals. The corresponding formula further increased the mineral content in order to avoid bone mineral density reduction problems that arise after weight loss in similar techniques.
    [00040] The integrated nutritional powder formula of this invention after many practices is constantly optimizing, taking into account the scope of the combination between the various elements, based on the mutual measures taken together and the respective functions of each component, not only for achieve rapid improvement in lifestyle diseases, but also promote improvement in general health. In addition, the conditioning process is comfortable and pain-free.
    [00041] The following are specific embodiments of the invention. IMPLEMENTED EXAMPLE 1
    [00042] The formula of the integrated nutritional powder is as follows:

    COMPARATIVE EXAMPLE 1
    [00043] The difference between comparative example 1 and implemented example 1 is the absence of Agaricus mushroom extract. COMPARATIVE EXAMPLE 2
    [00044] The difference between Comparative Example 2 and Implemented Example 1 is the absence of grape seed extract. EXPERIMENTAL EXAMPLE 1
    [00045] The person who underwent this treatment is called Ding Mou, he underwent a 6-week treatment, 5 times a day, each time he took 20g of the integrated nutritional powder of Implemented Example 1. During treatment, he avoided bad nutrition and practiced exercises regular.
    [00046] Table 1 of the hospital test result is below: Tongde Hospital - Zhejiang Province, intervention before detection time: 4 Aug 2011, No. 20110804LIB203; detection time after intervention: September 24, 2011, n° 20110924LIB158. After 6 weeks Ding Mou felt in a great state of mind.

    [00047] Test results can be seen above. The integrated nutritional powder of this invention reduces the weight of the obese, reduces fat, cholesterol etc., this has a significant effect. COMPARATIVE IMPLEMENTED EXAMPLE 1
    [00048] The person who underwent this treatment is called Liu Mou, he underwent a 6-week treatment, 5 times a day, each time he took 20g of the integrated nutritional powder from Comparative Example 1. During the treatment, he avoided poor diet and practiced regular exercise.
    [00049] Table 2 of the hospital test result is below: Tongde Hospital - Zhejiang Province, intervention before detection time: August 5, 2011, no. 20110805LIB103; detection time after intervention: September 24, 2011, n° 20110924LIB198. After 6 weeks Liu Mou felt fatigued.TABLE 2

    [00050] Test results can be seen above. The integrated nutritional powder of Comparative Example 1 reduces the obese weight, reduces fat, cholesterol etc., this has a significant effect. However, the person who has undergone this treatment feels more fatigued. In contrast, in test example 1, the user does not feel fatigued, because the Agaricus mushroom extract increases cellular activities, accelerates cell regeneration and tissue repair, thus increasing vitality.
    [00051] This written description uses examples to disclose the invention, including the best way and enabling the person skilled in the art to prepare and use this invention. The scope of the patent granted to the present invention is restricted by the claims and other examples can be presented by the expert in the field. If this other type of example contains structural elements of the literal language of the claims, or if this other example includes structural elements equivalent to the insubstantial differences of the literal language of the claims, such example is intended to be within the scope of the claims. When inconsistencies do not result, all references will be incorporated into the text by citation.
    权利要求:
    Claims (8)
    [0001]
    1. Integrated nutritional powder, characterized in that it contains the following elements, in percentage by weight: vitamin B1, 0.04; vitamin B2, 0.04, vitamin B6, 0.04, pantothenic acid, 0.04, nicotinic acid, 0.04; vitamin B12, 0.00004; vitamin C, 0.45; vitamin A, 0.0009; vitamin K, 0.000027, vitamin D, 0.0000113; vitamin E, 0.75; biotin, 0.00004; folic acid, 0.00059; calcium, 1.625; magnesium, 0.8125; iron, 0.027; zinc, 0.18; selenium, 0.00026; chromium, 0.0004; copper, 0.0022; manganese, 0.0045; corn fiber powder, 13; inulin, 8; isolated soy protein powder, 63; black bean husk extract, 6.25; Agaricus mushroom extract,3,75; soy lecithin, 12.5; red bean extract,3.75; L-carnitine, 0.648; β-carotene, 0.026; lycopene, 3; citrus extract, 0.648; vanadium, 0.00015; acerola extract, 7,776; grape seed extract, 0.7776; maltodextrin, 1-2; essence, 0.5-2; aspartame, 0.05-0.5; ethyl maltol 0.1-0.2 and acesulfame potassium 0.05-0.5.
    [0002]
    2. Nutritional powder according to claim 1, characterized in that the Agaricus mushroom extract contains at least 80% by weight of polysaccharide, where said polysaccharide has more than 80% by weight of protein binding, of the complex type (1^6) -β-D - dextran - protein element.
    [0003]
    Nutritional powder according to claim 1, characterized in that the acerola extract contains 5-15% by weight of 5-hydroxymethyl-furan-2-carbaldehyde and 50-70% by weight of proline.
    [0004]
    Nutritional powder according to claim 1, characterized in that the grape seed extract contains at least 35% by weight of oligomeric proanthocyanidins.
    [0005]
    5. Method for preparing the nutritional powder as defined in claim 1, characterized in that it comprises the following steps: (1) Mixing and size reduction by grinding vitamin B1, vitamin B2, vitamin B6, pantothenic acid, nicotinic acid, vitamin B12, vitamin C, vitamin A, vitamin K, vitamin D, vitamin E, biotin, folic acid, and inorganic salts of vanadium, calcium, magnesium, iron, zinc, selenium, chromium, copper and manganese in parts by weight in a blender. shear, the powder particle size should be less than 10μm, obtaining a first mixture; (2) The isolated soy protein powder and inulin must be uniformly mixed in the blender to obtain a second blend; (3)Corn fiber powder, black bean husk extract, Agaricus mushroom extract, soy lecithin, red bean extract, L-carnitine, β-carotene, lycopene, citrus extract, acerola extract, grape seed, maltodextrin, essence, aspartame, ethyl maltol and potassium acesulfame must be mixed together to obtain a third mixture, where the mixture of ethanol and acetone is added, stirring well until obtaining a liquid mixture, then going through a process spray drying or freeze drying to obtain a powdered product; and (4) Mix the first mixture, second mixture and said powdered product in a mixer for 15-30 min, pass through a 50-80 mesh sieve, sterilize in the microwave for 30-60min, package and inspect the final product nutritional powder.
    [0006]
    Method of preparation according to claim 5, characterized in that in step 3, the weight ratio of the third mixture and the ethanol is 1:31:10.
    [0007]
    Method of preparation according to claim 5, characterized in that in step 3, the volume of ethanol and acetone is 10:1-10:3.
    [0008]
    8. Method of preparation according to claim 5, characterized in that, before the extraction of the extract of the Agaricus mushroom, the fermentation of the Agaricus mushroom is carried out.
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    公开号 | 公开日
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    CA2944529A1|2016-02-11|
    BR112016016588A2|2018-06-05|
    CN104187624B|2016-06-08|
    MX2016008835A|2017-08-15|
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    DE102015100923A1|2016-02-11|
    CA2944529C|2018-07-31|
    RU2016132172A|2018-02-08|
    US20150140178A1|2015-05-21|
    EP3138414A4|2017-06-07|
    WO2016019597A1|2016-02-11|
    CN104187624A|2014-12-10|
    EP3138414A1|2017-03-08|
    RU2658365C2|2018-06-21|
    AU2014403009A1|2016-08-11|
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    法律状态:
    2018-06-12| B15I| Others concerning applications: loss of priority|
    2018-08-14| B12F| Other appeals [chapter 12.6 patent gazette]|
    2020-06-16| B06U| Preliminary requirement: requests with searches performed by other patent offices: procedure suspended [chapter 6.21 patent gazette]|
    2020-11-17| B06A| Patent application procedure suspended [chapter 6.1 patent gazette]|
    2021-03-30| B06A| Patent application procedure suspended [chapter 6.1 patent gazette]|
    2021-03-30| B15K| Others concerning applications: alteration of classification|Free format text: A CLASSIFICACAO ANTERIOR ERA: A23L 1/29 Ipc: A23L 33/00 (2016.01) |
    2021-05-11| B06A| Patent application procedure suspended [chapter 6.1 patent gazette]|
    2021-07-13| B09A| Decision: intention to grant [chapter 9.1 patent gazette]|
    2021-09-14| B16A| Patent or certificate of addition of invention granted [chapter 16.1 patent gazette]|Free format text: PRAZO DE VALIDADE: 20 (VINTE) ANOS CONTADOS A PARTIR DE 18/08/2014, OBSERVADAS AS CONDICOES LEGAIS. |
    优先权:
    申请号 | 申请日 | 专利标题
    CN2014103852291|2014-08-07|
    CN201410385229.1A|CN104187624B|2014-08-07|2014-08-07|Comprehensive nutrition powder and its preparation method|
    PCT/CN2014/084582|WO2016019597A1|2014-08-07|2014-08-18|Comprehensive nutrition powder and preparation method therefor|
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